2-Bromoanisole → HCID 178506687, compound

Participants

Reaction Conditions

Reaction Steps

2-Methoxybromobenzene (8.44 g 45.1 mmol) was dissolved in dry diethyl ether (15 mL). The mixture was cooled to −78° C. n-BuLi (17.8 mL, 45.0 mmol) was added and the mixture was stirred for one hour at −78° C. and then for 20 min. at −10° C. The aryl lithium solution was used immediately.

Provenance & Evidence