HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(1H-Indol-3-YL)cyclohexanone → 4-(2-Methyl-1H-3-indolyl)-cyclohexanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(1H-Indol-3-YL)cyclohexanone | HCID 10846264 | — |
| Edukt | 3-(1,4-dioxa-spiro[4,5]dec-8-yl)-2-methyl-1H-indole | HCID 18414099 | — |
| Produkt | 4-(2-Methyl-1H-3-indolyl)-cyclohexanone | HCID 18414056 | 88% |
Reaktionsschritte
This compound was prepared in the manner described above for intermediate 3a by replacing 3-(1,4-dioxa-spiro[4,5]dec-8-yl)-1H-indole with 3-(1,4-dioxa-spiro[4,5]dec-8-yl)-2-methyl-1H-indole (2.2 g) to afford 1.62 g (88%) of the title compound as a yellow thick oil: MS EI m/e 227 (M+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06313126B1 |
| Quelldatensatz | uspto-grants-2001_11 |
| ORD ID | ord-f89c8bdc5383465789076d38b682a162 |
| Quellennotiz | uspto-grants-2001_11 |