HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178519270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 178519269 | HCID 178519269 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178519270 | HCID 178519270 | — |
Reaction Steps
Sodium borohydride (10 mg) is added into a solution of 6-hydroxy-3-(1H-imidazol-4-ylmethyl)-indan-5-carbaldehyde (58 mg) in ethanol (10 ml). The mixture is stirred at room temperature for one hour and then poured into water. Work-up of the mixture gives the crude product which is purified by flash chromatography and recrystallized from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313311B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-5ff23d2c97ea4d1f970527d9a842914c |
| Source note | uspto-grants-2001_11 |