HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovanillin → HCID 18359237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | HCID 178462451 | HCID 178462451 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18359237 | HCID 18359237 | — |
Reaction Steps
3-Hydroxy-3-(3-hydroxy-4-methoxyphenyl)-1-propyne was prepared according to Method B above from 3-hydroxy-4-methoxybenzaldehyde (0.304 g, 2 mmol) (Aldrich) in THF (20 mL) and ethynylmagnesium chloride (5 mmol, 10 mL, 0.5M solution in tetrahydrofuran) (Aldrich). (Yield 273 mg, 77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313310B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-88f0a6109bed4b868483f6d1c3e5cd10 |
| Source note | uspto-grants-2001_11 |