反应详情

Caprolactam, which is commercially available, (10.0 g, 88.0 mmol), Et3N (14.8 mL, 106 mmol) and chlorotrimethylsilane (13.5 mL, 106 mmol) were dissolved in toluene (60 mL) and refluxed under Ar for 3 h. The reaction was filtered and concentrated to give the title compound.

1. temperaturerefluxed under Ar for 3 h
2. filtrationThe reaction was filtered
3. concentrationconcentrated