HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthylamine → HCID 18354528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthylamine | HCID 8640 | — |
| Reactant | 3-(4-Methylpiperazin-1-yl)-4-methoxybenzene sulfonyl chloride | HCID 54106808 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18354528 | HCID 18354528 | 67% |
Reaction Steps
1-Naphthylamine (29 mg, 0.2 mmol) was added to a stirred solution of 3-(4-methyl-1-piperazinyl)-4-methoxybenzene sulfonyl chloride (D2) (60 mg, 0.2 mmol) in acetone (1 ml) at ambient temperature. After stirring, for 18 h, the precipitate was filtered off and washed with acetone and diethyl ether to afford the title compound (E1) as a cream solid (60 mg, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316450B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-c22da2addc5b48629a246b385d0268bc |
| Source note | uspto-grants-2001_11 |