HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4'-(3-Chloropropoxy)[1,1'-biphenyl]-4-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4'-(3-chloropropoxy)[1,1'-biphenyl]-4-carboxylic Acid | HCID 18354759 | — |
| Product | 4'-(3-Chloropropoxy)[1,1'-biphenyl]-4-carbonyl chloride | HCID 18354766 | — |
Reaction Steps
The product from Example 10C (3.5 g, 11.36 mmol) in thionyl chloride (25 mL) was heated at 90° C. for 4 hours. The solution was allowed to cool to ambient temperature and then the mixture was evaporated to dryness to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316475B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-1ca31dc1e04a4b4b977477ae4000b2cf |
| Source note | uspto-grants-2001_11 |