HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 18355456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 18355455 | HCID 18355455 | — |
| Solvent | (+-)-2-Butanol | HCID 6568 | — |
| Product | HCID 18355456 | HCID 18355456 | — |
Reaction Steps
562 g of compound 6 are stirred at 85° C. in 900 g of 2-butanol and 50 ml of sulfuric acid for 5 hours. Cool down to room temperature. Filter the product. Wash twice with 100 ml of hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316487B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-87124c601c74420697bc1fa235218325 |
| Source note | uspto-grants-2001_11 |