HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15549582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4-Dichlorobenzenethiol | HCID 79964 | — |
| Reactant | 2-(2-Chloroethyl)-1-methylpyrrolidine | HCID 285093 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15549582 | HCID 15549582 | 43% |
Reaction Steps
2-(2-Chloroethyl)-1-methylpyrrolidine (1.50 g, 10.26 mmole), 3,4-dichlorobenzenethiol (1.82 g, 10.1 mmole), potassium carbonate (14.03 g, 101.6 mmole) and DMF (20 mL) were combined, yielding 0.46 g (4.34 mmole, 43%) of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316490B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-6d57402a2f694ec49d248f3020590e1a |
| Source note | uspto-grants-2001_11 |