HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 9816925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(2-Chloroethyl)-1-methylpyrrolidine | HCID 285093 | — |
| Reactant | HCID 13909774 | HCID 13909774 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9816925 | HCID 9816925 | — |
Reaction Steps
2-(2-Chloroethyl)-1-methylpyrrolidine (2.85 g, 19.29 mmole), 2-chloro-4-hydroxythiophenol (3.1 g, 19.29 mmole), potassium carbonate (26.7 g, 192.9 mmole) and DMF (30 mL) were combined, yielding 3.2 g (11.77 mmole, 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316490B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-9cccf8308e77455fa20f716db8e035e7 |
| Source note | uspto-grants-2001_11 |