HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131722991, compound → HCID 131722990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131722991 | HCID 131722991 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131722990 | HCID 131722990 | — |
Reaction Steps
(+,−) cis 7-Benzyloxy-4-[4-(morpholinoethyloxy)-phenyl]-3-phenyl-chroman (139 mg, 0.27 mmol) was dissolved in a solution of 1% hydrochloride in ethanol (5 ml). The solution was added to a 10% palladium on carbon catalyst, and hydrogenated (1 atm.) overnight. The reaction mixture was filtered and evaporated. The evaporated product was dissolved in acetone and evaporated to give a glassy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316494B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-1eed9305be0b4f22a9afc4b98c7be710 |
| Source note | uspto-grants-2001_11 |