HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanimidamide, hydrochloride (1:1) → HCID 178524252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanimidamide, hydrochloride (1:1) | HCID 10313058 | — |
| Reactant | HCID 18355342 | HCID 18355342 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178524252 | HCID 178524252 | 55.4% |
Reaction Steps
To a solution of ethyl 3-aminophthalic acid (1.00 g) in ethanol (10 ml) was added formamidine hydrochloride (444 mg) and refluxed for 12 hours. After cooling, the formed precipitate was collected by vacuum filtration and the precipitate was washed with ethanol to give 4-hydroxyquinazoline-5-carboxylic acid (504 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316482B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-f2df6bd751af49a08fc15fe6930748cc |
| Source note | uspto-grants-2001_11 |