HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 70076711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 4-Bromophenol | HCID 7808 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Product | HCID 70076711 | HCID 70076711 | 84.7% |
Reaction Steps
The title compound (6.22 g, 82%) was prepared from 4-bromophenol (5.0 g, 28.9 mmol), benzyl bromide (3.44 ml, 28.9 mmol) and cesium carbonate (10.36 g, 31.8 mmol) in a similar manner to Intermediate 76. 1H NMR (CDCl3) δ 7.50-7.30 (7H, m), 6.86 (2H, d, J 8.8 Hz) and 5.05 (2H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06319922B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-06368825befb4afd880fe80d2b43096f |
| Source note | uspto-grants-2001_11 |