HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-{2-[(Cyclohexylcarbonyl)amino]ethyl}-1-benzothiophene-5-carboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 70029514 | HCID 70029514 | — |
| Product | 3-{2-[(Cyclohexylcarbonyl)amino]ethyl}-1-benzothiophene-5-carboxylic acid chloride | HCID 88117951 | — |
Reaction Steps
5 mmol of the product obtained in Step F are dissolved in 40 ml of thionyl chloride. After stirring under an inert atmosphere for 1 hour, the thionyl chloride is removed by evaporation under reduced pressure to yield the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06319930B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-37034ab8394948128f460be90d81532b |
| Source note | uspto-grants-2001_11 |