Hydrochloric Acid → HCID 18353696, compound

Participants

Reaction Steps

The title compound was prepared according to the method described in Example 1(b) from 2-(2-aminomethylallylamino)-4-methoxyquinoline (70 mg, 0.29 mmol) and concentrated hydrochloric acid (2 mL) and was used without further purification. δH (CD3OD) 3.92 (2H, s), 4.53 (2H, s), 5.59 (2H, d, J=12.8), 6.61 (1H, d, J=0.9 Hz.), 7.65 (1H, dd, J=7.18 & 7.12 Hz), 7.93 (1H, dd, J=7.21 & 7.23 Hz), 8.02-8.16 (1H, m), 8.25 (1H, d, J=8.08 Hz); MS (ES+) 230 (31%) MH+ 213 (100%).

Provenance & Evidence