HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69708186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,4-Dioxa-8-azaspiro(4.5)decane | HCID 67435 | — |
| Reactant | HCID 18399769 | HCID 18399769 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 69708186 | HCID 69708186 | — |
Reaction Steps
A solution of 5 g of 3-(benzofuran-2-yl)-1-bromopropane, 3 g of 1, 4-dioxa-8-azaspiro[4.5]decane and 5.8 g of potassium carbonate in 200 ml of acetone is refluxed for 24 hours, and then evaporated to dryness. The residue is taken up in ethyl acetate, washed with water, dried and evaporated to yield the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06323217B2 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-b108c0e9eece43ceaba86f027af2141d |
| Source note | uspto-grants-2001_11 |