HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(N-Boc-amino)piperidine → HCID 70198275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(N-Boc-amino)piperidine | HCID 723833 | — |
| Reactant | HCID 18351359 | HCID 18351359 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 70198275 | HCID 70198275 | — |
Reaction Steps
A solution of 2.9 g of 3-(2-oxiranylmethyl)benzofuran, 4 g of tert-butyl 4-piperidyl-carbamate and 35 ml of isopropanol is heated at 80° C. for 5 hours. After evaporation to dryness, chromatography over silica gel enables the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06323217B2 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-ae51f488d57b42e1bfd672d56ac92dd8 |
| Source note | uspto-grants-2001_11 |