Hydrochloric Acid → HCID 18351344, compound

Participants

Reaction Conditions

Reaction Steps

A stream of hydrogen chloride gas is circulated through a solution of 3.64 g of the product obtained in Step A in 70 ml of ethanol. After 2 hours' stirring at 50° C., the reaction mixture is concentrated under reduced pressure. The residue is taken up in water and in 20% sodium hydroxide solution, extracted with dichloromethane, dried and then evaporated, enabling the expected product to be isolated.

Provenance & Evidence