HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → HCID 18351386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 18351353 | HCID 18351353 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18351386 | HCID 18351386 | — |
Reaction Steps
A mixture of 5.6 g of the product obtained in Step C, 3.7 g of ammonium formate and 0.56 g of 10% Pd/C in 120 ml of methanol is refluxed for 3 hours, then filtered over Celite and evaporated to dryness, enabling the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06323217B2 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-7c14a3e104914c16872d0a4dccd478a2 |
| Source note | uspto-grants-2001_11 |