HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloroformate → HCID 18351240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | HCID 18351238 | HCID 18351238 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18351240 | HCID 18351240 | — |
Reaction Steps
2-Amino-3-(4-phenylbenzoyl)-4,5,6,7-tetrahydrothieno(2,3-c)pyridine was reacted with benzyloxycarbonyl chloride and triethylamine to afford the title compound as a solid (mp 83-85° C.). 1H NMR (CDCl3) 2.05 (m, 2H); 3.45 (m, 2H); 4.46 (s, 2H); 5.15 (s, 2H); 6.72 (bs, 2H) 7.35-7.66 (m, 14H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06323214B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-e6b82c55577d40a48c57d0b9eb0a1fa7 |
| Source note | uspto-grants-2001_11 |