Sodium Iodide → HCID 22719916, compound

HRID 430635Notes

Reaction equation

HRID 430635 reaction equation
F[P-](F)(F)(F)(F)F.[CH3:8][N+:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][C:16]([C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1)=[O:17].[Na+].[I-:26]>CC(C)=O>[I-:26].[CH3:8][N+:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][C:16]([C:18]1[CH:19]=[CH:20][C:21]([CH3:24])=[CH:22][CH:23]=1)=[O:17]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 15487510HCID 15487510, compound

Product 1

HCID 22719916HCID 22719916, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

10 mmol of the compound obtained in Example 1 are dissolved in 35 ml of acetone, and 15 mmol of NaI are added in portions of 100 mg. A white precipitate is obtained immediately and the mixture is stirred for 14 hours in a sealed tube at ambient temperature.

Workup

  1. customA white precipitate is obtained immediately

Sources & evidence

ORD record
ord-2a8c9cd9cb0a4ff3827c45f80023a1f6
Source dataset
uspto-grants-2001_11
Patent number
US06323220B1

Reaction notes

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