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HRID430805

反应详情

EQUATION

反应方程式

HRID 430805 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)NC(=O)[C@@H](N)Cc1ccc(OCc2ccccc2)cc1
HCID15517727

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)NC(=O)[C@@H](N)Cc1ccc(OCc2ccccc2)cc1.Cl
HCID69584616

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

To a solution of (S)-2-amino-3-(4-benzyloxy-phenyl)-N-tert-butyl-propionamide (Example 1, Step B) in ether was added excess amount of ethereal HCl. The solid formed was isolated via filtration, and subsequent drying under vacuum gave (S)-2-Amino-3-(4-benzyloxy-phenyl)-N-tert-butyl-propionamide monohydrochloride as a yellow solid.

WORKUP

后处理

  1. customThe solid formed
  2. customwas isolated via filtration
  3. customsubsequent drying under vacuum