HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dioxolane-4-methanol, 2-ethyl-2-methyl- → HCID 18763754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dioxolane-4-methanol, 2-ethyl-2-methyl- | HCID 11804903 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18763754 | HCID 18763754 | 183.5% |
Reaction Steps
The compound obtained in the production (1) (29.2 g, 0.10 mol) and the palladium catalyst (2) (2.2 g) were charged in a 70-mL autoclave, followed by a reaction under a hydrogen pressure of 7.0MPa at 190° C. for 15 hours. After completion of the reaction, the catalyst was removed by filtration to obtain a crude product (27.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06657089B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-1a24222e394e4fd5aa78c72958a4dcd2 |
| Source note | uspto-grants-2003_12 |