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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 431305Generated: October 31, 2026

1,3-Dioxolane-4-methanol, 2-ethyl-2-methyl- → HCID 18763754, compound

https://huagongshe.com/reaction/431305

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-Dioxolane-4-methanol, 2-ethyl-2-methyl-HCID 11804903—
CatalystPalladiumHCID 23938—
ProductHCID 18763754HCID 18763754183.5%

Reaction Steps

The compound obtained in the production (1) (29.2 g, 0.10 mol) and the palladium catalyst (2) (2.2 g) were charged in a 70-mL autoclave, followed by a reaction under a hydrogen pressure of 7.0MPa at 190° C. for 15 hours. After completion of the reaction, the catalyst was removed by filtration to obtain a crude product (27.2 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06657089B1
Source datasetuspto-grants-2003_12
ORD IDord-1a24222e394e4fd5aa78c72958a4dcd2
Source noteuspto-grants-2003_12