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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 431371Generated: October 29, 2026

Hydrochloric Acid → HCID 59048191, compound

https://huagongshe.com/reaction/431371

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantLithium HydroxideHCID 3939—
ReactantHCID 69913671HCID 69913671—
SolventEthanolHCID 702—
SolventWaterHCID 962—
ProductHCID 59048191HCID 59048191—

Reaction Steps

A solution of LiOH (2.5 mmol) in water (1 ml) was added to 5-(2-pyridin-4-yl-vinyl)-isophthalic acid dimethylester (297 mg, 1 mmol) suspended in 5 ml EtOH. The mixture was stirred at room temperature. The reaction was monitored by TLC until completion. 2.5 ml 1 M HCl solution was then added and the mixture was evaporated to dryness. The product was used in next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06656971B2
Source datasetuspto-grants-2003_12
ORD IDord-1dea7b29f09343ac85a917ee49cdee22
Source noteuspto-grants-2003_12