Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trimethylamine → 1,3-Dihydroxy-5-trimethylsiloxyadamantane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trimethylamine | HCID 1146 | — |
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | 1,3,5-Adamantanetriol | HCID 9899022 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1,3-Dihydroxy-5-trimethylsiloxyadamantane | HCID 21930710 | — |
반응 단계
This 1,3,5-trihydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature. The reaction product was partitioned by high performance liquid chromatography to obtain 1,3-dihydroxy-5-trimethylsiloxyadamantane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06660450B2 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-609fd757932c4d9781e7d8b82ed4d6a3 |
| 출처 메모 | uspto-grants-2003_12 |