HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylamine → HCID 86585517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 21930705 | HCID 21930705 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86585517 | HCID 86585517 | — |
Reaction Steps
The 1,3-dichloroformyl-5-hydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature to obtain 1,3-dichloroformyl-5-trimethylsiloxyadamantane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06660450B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-0bf4edad633e4a898e3af4f4cb85a9d6 |
| Source note | uspto-grants-2003_12 |