HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54549583, compound → HCID 10107954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54549583 | HCID 54549583 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10107954 | HCID 10107954 | 70.3% |
Reaction Steps
0.846 g (3 mmol) of the product obtained in step d) were dissolved in 100 ml of dry ethanol. 150 mg of 10% palladium on charcoal were added, and the suspension was hydrogenated at 50° C. and 4 bar hydrogen pressure. After filtration the solvent was removed in vacuo. 0.6 g of a colourless oil were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06660728B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-074d49f404c746369c7bdb1fda0e1ba2 |
| Source note | uspto-grants-2003_12 |