Hydrochloric Acid → HCID 178524707, compound

HRID 432551Notes

Reaction equation

HRID 432551 reaction equation
[OH:1][C:2]1[C:15]2[C:6](=[C:7]3[C:12](=[CH:13][CH:14]=2)[C:11]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:10][CH:9]=[N:8]3)[N:5]=[CH:4][C:3]=1[C:22]([O:24]CC)=[O:23].[OH-].[Na+].Cl>>[OH:1][C:2]1[C:15]2[C:6](=[C:7]3[C:12](=[CH:13][CH:14]=2)[C:11]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:10][CH:9]=[N:8]3)[N:5]=[CH:4][C:3]=1[C:22]([OH:24])=[O:23]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 178469505HCID 178469505, compound

Product 1

HCID 178524707HCID 178524707, compound

Procedure

Ethyl 4-hydroxy-7-phenyl-1,10-phenanthroline-3-carboxylate (5.37 g) is boiled with 10% aqueous NaOH (32 mL) for 2 hours, acidified with 10% HCl to yield a precipitate that is collected, washed with water and dried to give the desired product.

Workup

  1. customto yield a precipitate that
  2. customis collected
  3. washwashed with water
  4. customdried

Sources & evidence

ORD record
ord-302a228c41884cd3a5c67fe955fe34d3
Source dataset
uspto-grants-2003_12
Patent number
US06664111B2

Reaction notes

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