HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbamate → HCID 18759809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbamate | HCID 77922 | — |
| Reactant | HCID 18759813 | HCID 18759813 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 18759809 | HCID 18759809 | — |
Reaction Steps
The BOC amine from 11A was dissolved in 4N HCl/dioxan (30 ml). The mixture was stirred at room temperature for 40 min then concentrated in vacuo to leave a tan solid; yield 0.41 g (63%, for 2 steps).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664249B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-c4b43dda80cd42598c4df9b9708dded5 |
| Source note | uspto-grants-2003_12 |