3-Nitrophenol → HCID 18760029, compound

Participants

Reaction Steps

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (106.9 mg, 0.327 mmol) and 3-nitrophenol were reacted as starting materials at 150° C. for 17 hours and post-treatment was then conducted, whereby the title compound was obtained as pale yellow prisms (140.4 mg, 99.9%). Melting point: 172.2-174.0° C. (ethyl acetate-diethyl ether-hexane).

Provenance & Evidence