2-Hydroxybenzonitrile → HCID 10112167, compound

Participants

Reaction Steps

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (110 mg, 0.337 mmol) and 2-cyanophenol were reacted as starting materials at 150° C. for 24 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow amorphous solid (121.4 mg, 88.1%). Melting point: 197.7-201.1° C. (ethyl acetate-hexane).

Provenance & Evidence