3-Cyanophenol → HCID 10294943, compound

Participants

Reaction Steps

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (175 mg, 0.536 mmol) and 3-cyanophenol were reacted as starting materials at 150° C. for 19 hours and post-treatment was then conducted, whereby the title compound was obtained as colorless prisms (165 mg, 75.2%). Melting point: 169.9-172.7° C. (ethyl acetate-diethyl ether-hexane).

Provenance & Evidence