HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Bis(4-methoxyphenyl)-6-chloropyridazine → HCID 18760033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Reactant | HCID 178418642 | HCID 178418642 | — |
| Product | HCID 18760033 | HCID 18760033 | — |
Reaction Steps
In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (200 mg, 0.613 mmol) and 4-hydroxypyridine were reacted as starting materials at 150° C. for 22 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow crystalline powder (201.6 mg, 85.2%). Melting point: 186.8-188.8° C. (hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-504710ad68b34f1c865cb401fbdaa054 |
| Source note | uspto-grants-2003_12 |