HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorophenol → HCID 10222036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorophenol | HCID 123051 | — |
| Reactant | HCID 18760010 | HCID 18760010 | — |
| Product | HCID 10222036 | HCID 10222036 | — |
Reaction Steps
In a similar manner as in Example 2, 6-chloro-3-(4-methoxyphenyl)-4-(4-pyridyl)pyridazine (150 mg, 0.504 mmol) and 2,4-difluorophenol were reacted as starting materials at 150° C. for 25 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow amorphous solid (157.0 mg, 79.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-ac96336e440b4aeebf1c9589554594f3 |
| Source note | uspto-grants-2003_12 |