HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentafluorophenol → HCID 10203873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentafluorophenol | HCID 13041 | — |
| Reactant | HCID 18760041 | HCID 18760041 | — |
| Product | HCID 10203873 | HCID 10203873 | — |
Reaction Steps
In a similar manner as in Example 2, 6-chloro-3-(4-methoxyphenyl)-4-phenylpyridazine (200 mg, 0.675 mmol) and 2,3,4,5,6-pentafluorophenol were reacted as starting materials at 150° C. for 48 hours and post-treatment was then conducted, whereby the title compound was obtained as a colorless crystalline powder (91.2 mg, 30.5%). Melting point: 133.1-133.9° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-49a67e3429584fc594a642f41da29076 |
| Source note | uspto-grants-2003_12 |