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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 432646Generated: October 31, 2026

Thiophenol → HCID 10185122, compound

https://huagongshe.com/reaction/432646

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThiophenolHCID 7969—
ReactantHCID 18760020HCID 18760020—
ProductHCID 10185122HCID 10185122—

Reaction Steps

In a similar manner as in Example 2, 6-chloro-4-(4-chlorophenyl)-3-[4-(methylthio)phenyl]pyridazine (150 mg, 0.303 mmol) and thiophenol (119 mg) were reacted as starting materials at 150° C. for 20 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow crystalline powder (85.0 mg, 39.8%). Melting point: 53.3-56.2° C.(diethyl ether-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06664256B1
Source datasetuspto-grants-2003_12
ORD IDord-fba8f2adb9e24c8da0b8bfa379f55994
Source noteuspto-grants-2003_12