HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorophenol → HCID 10297058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorophenol | HCID 123051 | — |
| Reactant | HCID 18760020 | HCID 18760020 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | HCID 10297058 | HCID 10297058 | — |
Reaction Steps
In a similar manner as in Example 2, 6-chloro-4-(4-chlorophenyl)-3-[4-(methylthio)phenyl]pyridazine (230.0 mg, 0.662 mmol) and 2,4-difluorophenol were reacted as starting materials at 150° C. for 20 hours and post-treatment was then conducted, whereby the title compound was obtained as colorless plates (dichloromethane-hexane, 216.2 mg, 74.0%). Melting point: 163.2-164.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-84f2adfd236f4e7682dc212d947aea6f |
| Source note | uspto-grants-2003_12 |