HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorophenol → HCID 18760030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorophenol | HCID 123051 | — |
| Reactant | HCID 18760019 | HCID 18760019 | — |
| Product | HCID 18760030 | HCID 18760030 | — |
Reaction Steps
In a similar manner as in Example 2, 6-chloro-3-(3,4-dimethoxyphenyl)-4-(4-methoxyphenyl)pyridazine (203 mg, 0.589 mmol) and 2,4-difluorophenol were reacted as starting materials at 150° C. for 20 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow amorphous solid (260 mg, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-7293b89d1a094a0f8c1639b9f679847c |
| Source note | uspto-grants-2003_12 |