HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 18760036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Product | HCID 18760036 | HCID 18760036 | — |
Reaction Steps
In a similar manner as in Example 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (300 mg, 0.918 mmol) and benzylamine were reacted as starting materials at 120° C. for 19 hours and post-treatment was then conducted, whereby the title compound was obtained as colorless prisms (365 mg, quantitative). Melting point: 125.4-126.3° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-2cdb8ca9b2a7439e847d9b33a328e7dc |
| Source note | uspto-grants-2003_12 |