HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluoroaniline → HCID 18760015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluoroaniline | HCID 9709 | — |
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Product | HCID 18760015 | HCID 18760015 | — |
Reaction Steps
In a similar manner as in Example 2, 3,4-bis-(4-methoxyphenyl)-6-chloropyridazine (264.2 mg, 0.809 mmol) and 2,4-difluoroaniline were reacted as starting materials at 100° C. for 12 hours and post-treatment was then conducted, whereby the title compound was obtained as a colorless crystalline powder (328.8 mg, 97.0%). Melting point: 177.4-178.0° C. (chloroform-diethyl ether-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-50ccb7e1c76b4f61aa977a142031a8e1 |
| Source note | uspto-grants-2003_12 |