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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 432654Generated: November 3, 2026

3,4-Bis(4-methoxyphenyl)-6-chloropyridazine → HCID 18759995, compound

https://huagongshe.com/reaction/432654

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4-Bis(4-methoxyphenyl)-6-chloropyridazineHCID 12568084—
ReactantHCID 18760017HCID 18760017—
ProductHCID 18759995HCID 18759995—

Reaction Conditions

Temperature100 °C

Reaction Steps

In a similar manner as in Example 2, 3,4-bis-(4-methoxyphenyl)-6-chloropyridazine (180 mg, 0.551 mmol) and N-(n-propyl)-2,4-difluoroaniline, as starting materials, were stirred 100° C. for 12 hours and then reacted at 170° C. for 10 hours, and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow-brown amorphous solid (137.5 mg, 54.1%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06664256B1
Source datasetuspto-grants-2003_12
ORD IDord-b8941993ba774d07be7d869f227eb5bb
Source noteuspto-grants-2003_12