HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4,5-Trimethoxyaniline → HCID 18759993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4,5-Trimethoxyaniline | HCID 32285 | — |
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Product | HCID 18759993 | HCID 18759993 | — |
Reaction Steps
In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (150.0 mg, 0.459 mmol) and 3,4,5-trimethoxy aniline were reacted as starting materials at 140° C. for 5 hours and post treatment was then conducted, whereby the title compound was obtained as a pale yellow crystalline powder (155.0 mg, 71.3%). Melting point: 125.4-126.3° C. (chloroform-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-b29f734cfa0747a1b8d642fa2711d452 |
| Source note | uspto-grants-2003_12 |