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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 432655Generated: October 31, 2026

3,4,5-Trimethoxyaniline → HCID 18759993, compound

https://huagongshe.com/reaction/432655

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4,5-TrimethoxyanilineHCID 32285—
Reactant3,4-Bis(4-methoxyphenyl)-6-chloropyridazineHCID 12568084—
ProductHCID 18759993HCID 18759993—

Reaction Steps

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (150.0 mg, 0.459 mmol) and 3,4,5-trimethoxy aniline were reacted as starting materials at 140° C. for 5 hours and post treatment was then conducted, whereby the title compound was obtained as a pale yellow crystalline powder (155.0 mg, 71.3%). Melting point: 125.4-126.3° C. (chloroform-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06664256B1
Source datasetuspto-grants-2003_12
ORD IDord-b29f734cfa0747a1b8d642fa2711d452
Source noteuspto-grants-2003_12