HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 18760016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Product | HCID 18760016 | HCID 18760016 | — |
Reaction Steps
In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (125.5 mg, 0.384 mmol) and morpholine were reacted as starting materials at 100° C. for 15 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow crystalline powder (115.2 mg, 79.5%). Melting point: 188.0-190.3° C. (chloroform-diethylether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-4c88ad9567b345a387933365c82498ce |
| Source note | uspto-grants-2003_12 |