HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18760173, compound → HCID 18760188, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18760173 | HCID 18760173 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18760188 | HCID 18760188 | 94.7% |
Reaction Steps
Using the general method of Example 3 Part B, 1-{2-[(3-thien-2-ylprop-2-ynyl)oxy]ethyl}-1H-imidazo[4,5-c]quinoline (9.5 g, 28.49 mmol) was reduced with palladium on carbon (10%, 1 g) in methanol (25 mL) to provide 9.1 g of 1-[2-(3-thien-2-ylpropoxy)ethyl]-1H-imidazo[4,5-c]quinoline as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664260B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-9d8776f1e7a440cbb52218b0704803f3 |
| Source note | uspto-grants-2003_12 |