HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → 1-tert-Butyl-3,3,5,5-tetraethylpiperazin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Ethyl ketone | HCID 7288 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18760498 | HCID 18760498 | — |
| Product | 1-tert-Butyl-3,3,5,5-tetraethylpiperazin-2-one | HCID 22182259 | 52% |
Reaction Steps
In analogy to Example B21, 1,1-diethyl-2-t-butylaminoethylamin, diethylketon, chloroform and NaOH are reacted to give the title compound (52%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664353B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-8d02224f77164396bdabc8ebde216447 |
| Source note | uspto-grants-2003_12 |