反应详情

11 mmol of tetrahydrothiophene was dissolved in 10 ml of dichloromethane at 0° C., and about 12 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. As a result, a white solid product in a salt form was obtained after about 5 minutes. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

1. customAs a result, a white solid product in a salt form was obtained after about 5 minutes
2. filtrationThe solid product was filtered
3. customdried for 1 hour in an oven at 50° C.
4. customto obtain the following product