反应详情

温度

40 °C

144.2 g of Octanoic Acid is charged at room temperature and heated to 40° C., then 154.64 g of Thionyl Chloride is added over a period of 1 hour and the reaction mixture is heated to reflux at 110° C. for 1½ hour to obtain crude Octanoyl Chloride.

1. temperaturethe reaction mixture is heated
2. temperatureto reflux at 110° C. for 1½ hour