Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Octanoic Acid | HCID 379 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Octanoyl chloride | HCID 8124 | — |
Reaction Steps
144.2 g of Octanoic Acid is charged at room temperature and heated to 40° C., then 154.64 g of Thionyl Chloride is added over a period of 1 hour and the reaction mixture is heated to reflux at 110° C. for 1½ hour to obtain crude Octanoyl Chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08536355B2 |
|---|
| Source dataset | uspto-grants-2013_09 |
|---|
| ORD ID | ord-a167b60b59f440498a8198b5d77db73e |
|---|
| Source note | uspto-grants-2013_09 |
|---|
