HuagongsheHuagongshe Chemistry Print Report · For research reference only
(R)-(-)-1-Methyheptyl 4-Methoxycarbonyloxybenzoate → (R)-(-)-1-Methylheptyl 4-Hydroxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (R)-(-)-1-Methyheptyl 4-Methoxycarbonyloxybenzoate | HCID 70010659 | — |
| Solvent | Ammonia | HCID 222 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | (R)-(-)-1-Methylheptyl 4-Hydroxybenzoate | HCID 13980124 | — |
Reaction Steps
Compound 3 (11.6 g, 38 mmol) in ethanol (200 ml) and aqueous ammonia (50 ml) was stirred overnight. The solvents were removed in vacuo and the resulting colourless oil was purified by column chromatography (ethyl acetate) on silica.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06666989B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-b0f16c51de7747f9ab721b7f67c9b915 |
| Source note | uspto-grants-2003_12 |