HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl tiglate → HCID 56949563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl tiglate | HCID 5281163 | — |
| Reactant | HCID 178418634 | HCID 178418634 | — |
| Product | HCID 56949563 | HCID 56949563 | — |
Reaction Steps
A mixture of 3.20 g (0.025 mol) of ethyl tiglate and 4.76 g (0.0625 mol) of thioacetic acid was prepared and allowed to react under nitrogen atmosphere at 85° C. for 24 hours. The results showed that the conversion rate of ethyl tiglate was 35.3%, and that the selectivity for the objective compound was 91.6%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536364B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-9a99f6c83ecb45f2a14080de6416e4b9 |
| Source note | uspto-grants-2013_09 |